In order to use segmented chemical flow processing in more complex reaction sequences, a method has been developed to precisely control the addition of reagent streams during multi-step operations. Using in-line infra-red monitoring with a new LabVIEW software application, it is possible to control additional pumps to dispense further reagents in real time based upon the concentration of reaction intermediates. This enables precise mixing with perfect timing thus greatly increasing product quality and enabling segmented chemical flow processing to be used in extended reaction sequences. © The Royal Society of Chemistry 2011.
A Breakthrough Method for the Accurate Addition of Reagents in Multi-step Segmented Flow Processing / Lange, Heiko; CARTER Catherine, F.; HOPKIN Mark, D.; Burke, Adrian; GOODE Jon, G.; BAXENDALE Ian, R.; LEY Steven, V.. - In: CHEMICAL SCIENCE. - ISSN 2041-6520. - 2:4(2011), pp. 765-769. [10.1039/c0sc00603c]
A Breakthrough Method for the Accurate Addition of Reagents in Multi-step Segmented Flow Processing
LANGE HeikoPrimo
;
2011
Abstract
In order to use segmented chemical flow processing in more complex reaction sequences, a method has been developed to precisely control the addition of reagent streams during multi-step operations. Using in-line infra-red monitoring with a new LabVIEW software application, it is possible to control additional pumps to dispense further reagents in real time based upon the concentration of reaction intermediates. This enables precise mixing with perfect timing thus greatly increasing product quality and enabling segmented chemical flow processing to be used in extended reaction sequences. © The Royal Society of Chemistry 2011.| File | Dimensione | Formato | |
|---|---|---|---|
|
Lange et al. Controlled flow_Chem. Sci. 2011, 2, 765-769.pdf
non disponibili
Descrizione: Articolo principale
Tipologia:
Documento in Post-print
Licenza:
Accesso privato/ristretto
Dimensione
475.94 kB
Formato
Adobe PDF
|
475.94 kB | Adobe PDF | Visualizza/Apri Richiedi una copia |
I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
