Full assignment of the H-1 and C-13 NMR spectra of ent-atisane-3 beta,16 alpha-diol, a cytotoxic diterpene isolated from the Caribbean sponge Spirastrella cunctatrix, was achieved by extensive use of two-dimensional NMR spectroscopy and spectral simulation. This is the first complete NMR characterization af an atisane terpene.
Complete H-1 and C-13 Nmr Assignment of Ent-3-beta,16-alpha-atisanediol, A Cytotoxic Diterpene Isolated From the Sponge Spirastrella Cunctatrix / Cafieri, Francesco; Fattorusso, Ernesto; Y., Mahajnah; Mangoni, Alfonso. - In: MAGNETIC RESONANCE IN CHEMISTRY. - ISSN 0749-1581. - STAMPA. - 33:(1995), pp. 286-289. [10.1002/mrc.1260330411]
Complete H-1 and C-13 Nmr Assignment of Ent-3-beta,16-alpha-atisanediol, A Cytotoxic Diterpene Isolated From the Sponge Spirastrella Cunctatrix
CAFIERI, FRANCESCO;FATTORUSSO, ERNESTO;MANGONI, ALFONSO
1995
Abstract
Full assignment of the H-1 and C-13 NMR spectra of ent-atisane-3 beta,16 alpha-diol, a cytotoxic diterpene isolated from the Caribbean sponge Spirastrella cunctatrix, was achieved by extensive use of two-dimensional NMR spectroscopy and spectral simulation. This is the first complete NMR characterization af an atisane terpene.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
